Butyl isocyanate → HCID 15550545, compound

HRID 2308361Notes

Reaction equation

HRID 2308361 reaction equation
[C:1]([C:5]1[CH:6]=[C:7]([CH:10]=[C:11]([C:14]([CH3:17])([CH3:16])[CH3:15])[C:12]=1[OH:13])[CH:8]=[O:9])([CH3:4])([CH3:3])[CH3:2].[CH2:18]([N:22]=[C:23]=[O:24])[CH2:19][CH2:20][CH3:21]>CN(C=O)C>[CH2:18]([NH:22][C:23]([O:13][C:12]1[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])=[CH:6][C:7]([CH:8]=[O:9])=[CH:10][C:11]=1[C:14]([CH3:17])([CH3:16])[CH3:15])=[O:24])[CH2:19][CH2:20][CH3:21]

Participants

4

Reactant 2

HCID 8110Butyl isocyanateHCID 732193,5-Di-tert-butyl-4-hydroxybenzaldehyde

Product 1

HCID 15550545HCID 15550545, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

The title compound was prepared in DMF using 3,5-di-tert-butyl-4-hydroxybenzaldehyde and n-butyl isocyanate according to the procedure described in Example H. The title compound was isolated in 87.5% yield as a buff solid.

Sources & evidence

ORD record
ord-882dba81765c495f876e4e6e36d8c28d
Source dataset
uspto-grants-2004_12
Patent number
US06835754B2

Reaction notes

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