HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fluorine → HCID 12994024, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fluorine | HCID 24524 | — |
| Reactant | Octanoyl fluoride, 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro- | HCID 67634 | — |
| Reactant | 1,2-Dichloro-1,1,2-trifluoro-2-(trifluoromethoxy)ethane | HCID 102791 | — |
| Product | HCID 12994024 | HCID 12994024 | — |
Reaction Steps
19.65 g of CF3—OCFCl—CF2Cl as solvent, 23.07 g of CFCl═C—FCl (CFC 1112) and 7.57 g of CF3—(CF2)6—COF are introduced into the equipment described in the Example 1. The reaction mixture is maintained at the temperature of −55° C. and 1.5 Nl/h of fluorine diluted with nitrogen (molar ratio fluorine/nitrogen 1/5) are fed therein for 110 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835856B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-a61d3ca5930a493e97e19c10bca479f2 |
| Source note | uspto-grants-2004_12 |