HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-nitroanisole → HCID 86584952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-nitroanisole | HCID 118533 | — |
| Reactant | HCID 10014834 | HCID 10014834 | — |
| Reactant | HCID 10155956 | HCID 10155956 | — |
| Product | HCID 86584952 | HCID 86584952 | — |
Reaction Steps
The title compound was prepared strarting from 4-bromo-1-methoxy-2-nitro-benzene and trimethyl-thiophen-3-yl-stannane as described for morpholine-4-carboxylic acid (4-methoxy-7-phenyl-benzothiazol-2-yl)-amide (Example 157) and obtained as a light yellow solid in about 10% overall yield, MS: m/e=376 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835732B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-95549267b5864cbdb5557fe459b412b8 |
| Source note | uspto-grants-2004_12 |