HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → (5-Methoxy-biphenyl-3-yl)-thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | 1-Benzoyl-3-(5-methoxy-biphenyl-3-yl)-thiourea | HCID 22283319 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | (5-Methoxy-biphenyl-3-yl)-thiourea | HCID 22283392 | 88% |
Reaction Steps
1-Benzoyl-3-(5-methoxy-biphenyl-3-yl)-thiourea (183 mg, 0.51 mmol) in methanol (5 ml) are treated with sodium methoxide (5.4M in methanol, 0.14 ml) and the formed precipitate is filtered off. Washing with methanol yields the product (115 mg, 88%) as off-white powder. MS: m/e=258 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06835732B2 |
| Source dataset | uspto-grants-2004_12 |
| ORD ID | ord-1da8584fab624b88867a2bcf25ae0559 |
| Source note | uspto-grants-2004_12 |