Piperazine → HCID 20150137, compound

HRID 2308626Notes

Reaction equation

HRID 2308626 reaction equation
Cl[C:2]1[N:3]=[C:4]([N:19]2[CH2:24][CH2:23][S:22][CH2:21][CH2:20]2)[C:5]2[N:11]=[CH:10][N:9]=[C:8]([S:12][C:13]3[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=3)[C:6]=2[N:7]=1.[NH:25]1[CH2:30][CH2:29][NH:28][CH2:27][CH2:26]1>>[C:13]1([S:12][C:8]2[C:6]3[N:7]=[C:2]([N:25]4[CH2:30][CH2:29][NH:28][CH2:27][CH2:26]4)[N:3]=[C:4]([N:19]4[CH2:24][CH2:23][S:22][CH2:21][CH2:20]4)[C:5]=3[N:11]=[CH:10][N:9]=2)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 4837PiperazineHCID 20150125HCID 20150125, compound

Product 1

HCID 20150137HCID 20150137, compound

Procedure

This compound was prepared analogous to Example 2 from 2-chloro-8-phenylthio-4-thiomorpholino-pyrimido-[5,4-d]-pyrimidine (m.p.: 236°-238° C.) and piperazine.

Sources & evidence

ORD record
ord-50f079a032d44d4687874b9600ec208b
Source dataset
uspto-grants-1987_09
Patent number
US04690923

Reaction notes

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