HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl bromide → HCID 178419250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl bromide | HCID 68176 | — |
| Reactant | HCID 178520361 | HCID 178520361 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178419250 | HCID 178419250 | — |
Reaction Steps
Stir 600 mg of the product of Step A and 1.1 g thionyl bromide in 6 ml of chloroform under a nitrogen atmosphere for 11/2 hours. Evaporate the solvent in vacuo. Dry the resultant residue under high vacuum for 15 minutes to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04690922 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-bfbf273b6213466babd05bf54728a2af |
| Source note | uspto-grants-1987_09 |