HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione → 105441-18-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8,8-Trimethyl-3-oxabicyclo[3.2.1]octane-2,4-dione | HCID 94834 | — |
| Reactant | Homocysteine thiolactone hydrochloride | HCID 110753 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 105441-18-7 | HCID 3064724 | — |
Reaction Steps
According to the same procedure, 10 g (65 mmol) of DL-homocysteine thiolactone hydrochloride, 11.52 g (63 mmol) of DL-camphoric anhydride and 5.46 g (65 mmol) of NaHCO3 in 42 ml of CH2Cl2 and 1 ml of H2O were reacted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04690944 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-eb299631771842fcb18a1c9a3c3eac7a |
| Source note | uspto-grants-1987_09 |