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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2308714Generated: November 2, 2026

Hydrochloric Acid → HCID 13958008, compound

https://huagongshe.com/reaction/2308714

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 3387567HCID 3387567—
SolventWaterHCID 962—
ProductHCID 13958008HCID 1395800840%

Reaction Steps

3-(2-Phenylacetyl)-2-oxindole was acetylated with acetic anhydride using the procedure of Example 7. When the reaction mixture was poured into a mixture of 3N hydrochloric acid and water, a solid formed. The solid was recovered by filtration and recrystallized from isopropanol to give a 40% yield of the title compound, m.p. 149°-151° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04690943
Source datasetuspto-grants-1987_09
ORD IDord-e708f0f40f55468099619cbc9aeb1c25
Source noteuspto-grants-1987_09