HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 45258253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2-Bromopropiophenone | HCID 16452 | — |
| Reactant | 4-Benzylpiperidine | HCID 31738 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 45258253 | HCID 45258253 | — |
Reaction Steps
17.5 g (0.1 mol) of 4-benzylpiperidine and then 12 g of sodium carbonate are added to a solution of 21.3 g (0.1 mol) of 2-bromopropiophenone in 100 ml of ethanol, and the mixture is heated under reflux for 2 hours. It is then filtered and the solvent is driven off. An oil remains, which is used as such in the subsequent reduction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04690931 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-fba660146e1340f4aa25db3646c0bd2a |
| Source note | uspto-grants-1987_09 |