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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 230876Generated: October 30, 2026

Water → HCID 67136322, compound

https://huagongshe.com/reaction/230876

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantBenzyl BromideHCID 7498—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 67135797HCID 67135797—
SolventDimethylformamideHCID 6228—
ProductHCID 67136322HCID 67136322—

Reaction Steps

To a solution of 4′,6′-dihydroxy-2′-(methoxycarbonylmethoxy)dihydrochalcone (0.6 g) in N,N-dimethylformamide (10 mL) were added potassium carbonate (0.26 g) and benzyl bromide (0.22 mL), and the mixture was stirred at room temperature for 3 days. The reaction mixture was poured into water, and the precipitated crystals were collected by filtration and dried under reduced pressure to give the title compound (0.53 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07566699B2
Source datasetuspto-grants-2009_07
ORD IDord-98a75bf40fb341b28759c5935a5b86ad
Source noteuspto-grants-2009_07