HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 67136322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 67135797 | HCID 67135797 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67136322 | HCID 67136322 | — |
Reaction Steps
To a solution of 4′,6′-dihydroxy-2′-(methoxycarbonylmethoxy)dihydrochalcone (0.6 g) in N,N-dimethylformamide (10 mL) were added potassium carbonate (0.26 g) and benzyl bromide (0.22 mL), and the mixture was stirred at room temperature for 3 days. The reaction mixture was poured into water, and the precipitated crystals were collected by filtration and dried under reduced pressure to give the title compound (0.53 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07566699B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-98a75bf40fb341b28759c5935a5b86ad |
| Source note | uspto-grants-2009_07 |