HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 2-[(2-Chloro-6-hydrazinylphenyl)methyl]-4,4-dimethyl-1,2-oxazolidin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 2-[(2-Chloro-6-hydrazinophenyl)methyl]-4,4-dimethyl-3-isoxazolidinone hydrochloride | HCID 13934947 | — |
| Product | 2-[(2-Chloro-6-hydrazinylphenyl)methyl]-4,4-dimethyl-1,2-oxazolidin-3-one | HCID 13934946 | — |
Reaction Steps
The free hydrazine was obtained by treating of the yellow solid with aqueous sodium hydroxide. The mixture was extracted with ethyl acetate, and the extract was concentrated under reduced pressure to yield the free hydrazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04692182 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-a865dbd9beac42ad86d62507da12d43b |
| Source note | uspto-grants-1987_09 |