HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Piperazinecarboxylic acid, ethyl ester → HCID 13957256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Piperazinecarboxylic acid, ethyl ester | HCID 8431 | — |
| Reactant | 5,8-Quinoxalinedione | HCID 11355645 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 13957256 | HCID 13957256 | 47.5% |
Reaction Steps
A mixture of 160 mg of 5,8-quinoxalinedione and 316 mg of 1-piperazinecarboxylic acid ethyl ester in 10 ml of dioxane was stirred for 3 hours. The resulting solid was collected, washed with ether and dried, giving 150 mg of the desired product as a red solid, mp 180°-195° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04692449 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-3de90c4c43e24e7282bc5b9440e6243c |
| Source note | uspto-grants-1987_09 |