Ethylenediamine → HCID 10583474, compound

HRID 2308969Notes

Reaction equation

HRID 2308969 reaction equation
[CH2:1]([NH2:4])[CH2:2][NH2:3].[C:5]1([CH2:11][C:12](OCC)=[O:13])[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.NCC(N)(C)C>C(OCC)(=O)C>[C:5]1([CH2:11][C:12]([NH:3][CH2:2][CH2:1][NH2:4])=[O:13])[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1

Participants

5

Reactant 3

HCID 3301EthylenediamineHCID 7590Ethyl phenylacetateHCID 131282-Methylpropylenediamine

Product 1

HCID 10583474HCID 10583474, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The procedure of Example IX was repeated in all essential details to produce the above compound, except that equivalent amounts of ethylenediamine and ethyl phenylacetate were substituted for 1,2-diamino-2-methylpropane and ethyl acetate, respectively. The product, which was identified by NMR and IR spectroscopy, had a melting point of 37°-38° C.

Workup

  1. customto produce the above compound

Sources & evidence

ORD record
ord-fd5a694aa4df4c89a937cecc468cae41
Source dataset
uspto-grants-1987_09
Patent number
US04692446

Reaction notes

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