1-Decanol → Decane

HRID 2309108Notes

Reaction equation

HRID 2309108 reaction equation
[C:1]1([CH2:7][C:8]2(O)C3C[CH:11]4[CH2:12][CH:13](C[CH:9]2[CH2:10]4)C3)C=CC=[CH:3][CH:2]=1.C(O)CCCCCCCCC>>[CH3:3][CH2:2][CH2:1][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 81741-DecanolHCID 3752505HCID 3752505, compound

Product 1

HCID 15600Decane

Procedure

1-Chlorosulfonyl-3-phenyl-spiro[azetidin-2-one-4,2'-tricyclo[3.3.1.13,7 ]decane] (Compound A) was prepared by first synthesizing 2-(phenylmethyl)-tricyclo[3.3.1.13,7 ]decan-2-ol and dehydrating this decanol compound to form 2-(phenylmethylene)-tricyclo[3.3.1.3,7 ]decane in accordance with the following procedure:

Sources & evidence

ORD record
ord-f1a27700c78f40089d659a5e72c3a53d
Source dataset
uspto-grants-1987_09
Patent number
US04692515

Reaction notes

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