HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19360856, compound → Acenaphthene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19360856 | HCID 19360856 | — |
| Catalyst | 4-Phenoxybenzoyl chloride | HCID 74193 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | Acenaphthene | HCID 6734 | — |
Reaction Steps
In a small vial, about 200 mg (12 drops) of crude p-phenoxybenzoyl chloride is dissolved in about 2 ml of trifluoroacetic acid. To this yellowish-brown solution is added three drops of 5 wt % acenaphthene/dichloromethane solution. The vial is swirled to mix the contents thoroughly and the color is immediately observed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04693851 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-b831057a6d1847769381f1a6662be84e |
| Source note | uspto-grants-1987_09 |