Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Valeronitrile | HCID 8061 | — |
| Catalyst | Cadmium acetate, dihydrate | HCID 6537495 | — |
| Product | 2-n-Butyl-2-oxazoline | HCID 12209630 | — |
Reaction Steps
A mixture of about 83.1 grams (1.00 mole) valeronitrile, about 64.8 grams (1.05 mole) ethanolamine, and about 6.2 grams (0.025 mole) cadmium acetate dihydrate is heated at about 124 degrees C. to about 128 degrees C. and stirred under nitrogen for about two days. The product is then distilled under vacuum. The fraction boiling at about 67 degrees C. to about 75.5 degrees C. at about 28 mmHg is collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04695295 |
|---|
| Source dataset | uspto-grants-1987_09 |
|---|
| ORD ID | ord-68da6a0672f442fda88c211acb5feef7 |
|---|
| Source note | uspto-grants-1987_09 |
|---|
