反应详情

温度

115 °C

A mixture of about 50.g grams (0.515 mole) isoamyl cyanide, about 31.5 grams (0.515 mole) ethanolamine, and about 3.2 grams (0.012 mole) cadmium acetate dihydrate is heated to about 115 degrees C. to about 125 degrees C. and stirred under nitrogen for about two days. The product is distilled under vacuum and the fraction boiling at about 81 degrees C. to about 84 degrees C. at about 29 mmHg is collected.

1. customto about 125 degrees C
2. distillationThe product is distilled under vacuum
3. customto about 84 degrees C
4. customat about 29 mmHg is collected