Ethanolamine → HCID 12353703, compound

HRID 2309310Notes

Reaction equation

HRID 2309310 reaction equation
[CH2:1]([C:8]#[N:9])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7].[CH2:10]([CH2:12]N)[OH:11]>O.O.C([O-])(=O)C.[Cd+2].C([O-])(=O)C>[CH2:1]([C:8]1[O:11][CH2:10][CH2:12][N:9]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 700EthanolamineHCID 31286Octanenitrile

Product 1

HCID 12353703HCID 12353703, compound

Reagents, catalysts & solvents 1

HCID 6537495Cadmium acetate, dihydrateCatalyst

Conditions

Temperature
120 °C

Procedure

A mixture of about 100.0 grams (0.774 mole) of heptylcyanide, about 47.3 grams (0.774 mole) ethanolamine, and about 4.8 grams (0.019 mole) cadmium acetate dihydrate is heated to about 120 degrees C. to about 130 degrees C. for about 2 days. The mixture is distilled under vacuum and the fraction boiling at about 109 degrees C. to about 116 degrees C. at about 28 mmHg is collected for later use.

Workup

  1. customto about 130 degrees C
  2. distillationThe mixture is distilled under vacuum
  3. customto about 116 degrees C
  4. customat about 28 mmHg is collected for later use

Sources & evidence

ORD record
ord-d89367afd33f4d4d833835d887cbaf8b
Source dataset
uspto-grants-1987_09
Patent number
US04695295

Reaction notes

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