Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Octanenitrile | HCID 31286 | — |
| Catalyst | Cadmium acetate, dihydrate | HCID 6537495 | — |
| Product | HCID 12353703 | HCID 12353703 | — |
Reaction Steps
A mixture of about 100.0 grams (0.774 mole) of heptylcyanide, about 47.3 grams (0.774 mole) ethanolamine, and about 4.8 grams (0.019 mole) cadmium acetate dihydrate is heated to about 120 degrees C. to about 130 degrees C. for about 2 days. The mixture is distilled under vacuum and the fraction boiling at about 109 degrees C. to about 116 degrees C. at about 28 mmHg is collected for later use.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04695295 |
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| Source dataset | uspto-grants-1987_09 |
|---|
| ORD ID | ord-d89367afd33f4d4d833835d887cbaf8b |
|---|
| Source note | uspto-grants-1987_09 |
|---|
