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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 2309404Erstellt: 25. Oktober 2026

Einecs 211-027-4 → 2,6-Dimethyl-4-(3-methyl-1H-indol-2-yl)phenol

https://huagongshe.com/reaction/2309404

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEinecs 211-027-4HCID 69401—
Edukt2-(4-Methoxy-3,5-dimethylphenyl)-3-methylindoleHCID 13670141—
LösungsmittelWaterHCID 962—
Produkt2,6-Dimethyl-4-(3-methyl-1H-indol-2-yl)phenolHCID 1367014263,8%

Reaktionsschritte

4.3 g of 2-(4-methoxy-3,5-dimethylphenyl)-3-methylindole and 13 g of pyridinium chloride were reacted at 200° C. for 1.5 hours. The reaction mixture was cooled, poured into water, extracted with ethyl acetate, washed with water, and dried. The solvent was evaporated, and the residue was recrystallized from benzene-hexane to give 2.6 g of 2-(4-hydroxy-3,5-dimethylphenyl)-3-methylindole.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04695581
Quelldatensatzuspto-grants-1987_09
ORD IDord-b3a29044874c44b495ff169bdfa34147
Quellennotizuspto-grants-1987_09