HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Einecs 211-027-4 → 2,6-Dimethyl-4-(3-methyl-1H-indol-2-yl)phenol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Einecs 211-027-4 | HCID 69401 | — |
| Edukt | 2-(4-Methoxy-3,5-dimethylphenyl)-3-methylindole | HCID 13670141 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2,6-Dimethyl-4-(3-methyl-1H-indol-2-yl)phenol | HCID 13670142 | 63,8% |
Reaktionsschritte
4.3 g of 2-(4-methoxy-3,5-dimethylphenyl)-3-methylindole and 13 g of pyridinium chloride were reacted at 200° C. for 1.5 hours. The reaction mixture was cooled, poured into water, extracted with ethyl acetate, washed with water, and dried. The solvent was evaporated, and the residue was recrystallized from benzene-hexane to give 2.6 g of 2-(4-hydroxy-3,5-dimethylphenyl)-3-methylindole.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04695581 |
| Quelldatensatz | uspto-grants-1987_09 |
| ORD ID | ord-b3a29044874c44b495ff169bdfa34147 |
| Quellennotiz | uspto-grants-1987_09 |