HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Di-dodecyl 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Reactant | 3-(Benzothiazol-2-ylthio)-propane-1,2-dicarboxylic acid | HCID 19427537 | — |
| Product | Di-dodecyl 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylate | HCID 20184317 | — |
Reaction Steps
125 parts of dodecan-1-ol are saturated with dry hydrogen chloride gas at room temperature. 13.5 parts of 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylic acid are then added and the mixture heated to 85°. The resulting solution is stirred for 4 hours at 85°. Excess dodecan-1-ol is removed by heating at 90° under a vacuum of 0.01 mm Hg to give di-dodecyl 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylate as a yellow liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04696763 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-e8239de3893b4a81920403267dcff34b |
| Source note | uspto-grants-1987_09 |