反应详情

125 parts of dodecan-1-ol are saturated with dry hydrogen chloride gas at room temperature. 13.5 parts of 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylic acid are then added and the mixture heated to 85°. The resulting solution is stirred for 4 hours at 85°. Excess dodecan-1-ol is removed by heating at 90° under a vacuum of 0.01 mm Hg to give di-dodecyl 3-(benzothiazol-2-ylthio)-propane-1,2-dicarboxylate as a yellow liquid.

1. temperaturethe mixture heated to 85°
2. customExcess dodecan-1-ol is removed
3. temperatureby heating at 90° under a vacuum of 0.01 mm Hg