HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 12045651, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Benzyloxyamine hydrochloride | HCID 102312 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 12045651 | HCID 12045651 | — |
Reaction Steps
A mixture of 13.04 g of benzyloxyaminehydrochloride, 20.0 ml of benzylbromide, and 32.0 g of sodium carbonate in 85 ml of dimethylformamide is stirred at room temperature for four days. The reaction mixture is worked up as in Example I and the crude product is distilled under reduced pressure to afford the title compound as a clear colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04696964 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-86200743de9c4ea9ad5893948d7e1639 |
| Source note | uspto-grants-1987_09 |