Sodium Acetate → HCID 53929080, compound

HRID 230986Notes

Reaction equation

HRID 230986 reaction equation
[C:1]([CH:6]1[C:11](=[O:12])[CH2:10][CH:9]([C:13]2[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][CH:14]=2)[CH2:8][C:7]1=[O:20])(=O)[CH2:2][CH2:3][CH3:4].[Cl-].[CH2:22]([O:24][NH3+:25])[CH3:23].C([O-])(=O)C.[Na+]>C(O)C>[CH2:22]([O:24][NH:25][CH2:4][CH2:3][CH2:2][CH:1]=[C:6]1[C:11](=[O:12])[CH2:10][CH:9]([C:13]2[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][CH:14]=2)[CH2:8][C:7]1=[O:20])[CH3:23]

Participants

5

Reactant 3

HCID 517045Sodium AcetateHCID 19001768HCID 19001768, compoundHCID 20034300HCID 20034300, compound

Product 1

HCID 53929080HCID 53929080, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

13.5 parts of 2-butyryl-5-(4-chlorophenyl)-cyclohexane-1,3-dione, 4.5 parts by weight of ethoxyammonium chloride, 4.5 parts by weight of anhydrous sodium acetate and 100 parts by volume of ethanol are reacted, and the mixture is worked up, in a manner similar to that in Example 1. 2-(Ethoxyaminobutylidene)-5-(4-chlorophenyl)-cyclohexane-1,3-dione is obtained as a solid, which is recrystallized from cyclohexane. The product has a melting point of 77° C. (active ingredient No. 2)

Sources & evidence

ORD record
ord-ddb082b4a8684aa6b78acba86397c06b
Source dataset
uspto-grants-1989_07
Patent number
US04844735

Reaction notes

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