Sodium Acetate → HCID 53929080, compound

Participants

Reaction Steps

13.5 parts of 2-butyryl-5-(4-chlorophenyl)-cyclohexane-1,3-dione, 4.5 parts by weight of ethoxyammonium chloride, 4.5 parts by weight of anhydrous sodium acetate and 100 parts by volume of ethanol are reacted, and the mixture is worked up, in a manner similar to that in Example 1. 2-(Ethoxyaminobutylidene)-5-(4-chlorophenyl)-cyclohexane-1,3-dione is obtained as a solid, which is recrystallized from cyclohexane. The product has a melting point of 77° C. (active ingredient No. 2)

Provenance & Evidence