HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → N-Butyl-3-methoxy-4-(7H-purin-8-yl)benzene-1-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | HCID 20184500 | HCID 20184500 | — |
| Product | N-Butyl-3-methoxy-4-(7H-purin-8-yl)benzene-1-sulfonamide | HCID 13284538 | — |
Reaction Steps
Prepared analogously to Example 51 from n-butylamine and 8-(2'-methoxy-4'-chlorosulfonyl-phenyl)-purine hydrochloride. After the reaction finished, the aqueous phase wsa extracted with ethyl acetate. The residue remaining after the ethyl acetate phases were evaporated was digested with ethanol, subjected to suction filtration, and washed with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04696931 |
| Source dataset | uspto-grants-1987_09 |
| ORD ID | ord-be112d36ebf34269bb4d9373b5ffe902 |
| Source note | uspto-grants-1987_09 |