HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2309906Generated: October 31, 2026
HCID 20184509, compound → HCID 20184521, compound
https://huagongshe.com/reaction/2309906
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 20184509 | HCID 20184509 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 20184521 | HCID 20184521 | — |
Reaction Steps
Five grams (13.3 mmol) of 5-acetamino-2-(2'-methoxy-4'-methanesulfonyloxy-phenyl)-benzimidazole were suspended in 150 ml of concentrated hydrochloric acid and stirred at 80° C. for two hours. After cooling, the crude product precipitated was subjected to suction filtration and chromatographed on 500 gm of aluminium oxide (neutral) (eluant: methylene chloride with 2.5% ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04696931 |
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| Source dataset | uspto-grants-1987_09 |
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| ORD ID | ord-4710495d79344d1583bc71cc402bb8cd |
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| Source note | uspto-grants-1987_09 |
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