Acetylethylenimine → HCID 20034384, compound

Participants

Reaction Steps

13.3 g. (0.1 mol) 1,2,3,4-tetrahydroquinoline and 9.4 g. (0.11 mol) acetylaziridine were boiled overnight under reflux in 200 ml. anhydrous methanol. After evaporating in a rotary evaporator, the mixture obtained of unreacted starting material and reaction product (13 g.) was purified by column chromatography on silica gel (elution agent: chloroform/acetone=4/1 v/v; m.p. 102° C.

Provenance & Evidence