HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 14154362, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 14154328 | HCID 14154328 | — |
| Reactant | HCID 20034625 | HCID 20034625 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14154362 | HCID 14154362 | — |
Reaction Steps
1.1 g (3 mmol) of the title compound from Example 23 were dissolved in 50 ml of CH2Cl2, and 50 ml of the KH2PO4 /Na2HPO4 buffer solution from Example 22 were added. At 10° C. a total of 900 mg (4.5 mmol) of m-chloroperbenzoic acid in CH2Cl2 was added dropwise in portions until the precursor has been completely used up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845118 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-fa6af096bc5b4ea8b2b2bd9afe5eaac9 |
| Source note | uspto-grants-1989_07 |