HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenyl chloroformate → HCID 14154330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| Reactant | HCID 14014797 | HCID 14014797 | — |
| Solvent | Toluene ethylacetate | HCID 21584019 | — |
| Product | HCID 14154330 | HCID 14154330 | — |
Reaction Steps
The title compound was prepared in analogy to Example 17 from 2-(5-methyl-2-picolylmercapto)-1H-thieno[3,4-d]imidazole and p-nitrophenyl chloroformate. After working up and chromatography on silica gel using toluene/ethyl acetate (1:1), the appropriate fractions were crystallized from ethyl acetate, and the title compound was obtained. Melting point 165°-168° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845118 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-eda4355aae754c7fa6ee8def2c467481 |
| Source note | uspto-grants-1989_07 |