HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetamide → HCID 13632728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetamide | HCID 7898 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 13632725 | HCID 13632725 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13632728 | HCID 13632728 | — |
Reaction Steps
2-Acetyl-4-phenylcyclohexanone, 1.68 g, 0.73 g of cyanoacetamide and a small quantity of piperidine were mixed with 10 ml of ethanol followed by heating to reflux for 2 hours. After cooling, the precipitated crystals were taken out by filtration and purified to give 1.5 g of 4-cyano-2,3,5,6,7,8-hexahydro-1-methyl-3-oxo-7-phenylisoquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845228 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-5a55308ca9754ff68b1b8fdce636e4c4 |
| Source note | uspto-grants-1989_07 |