HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 14498242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 20034841 | HCID 20034841 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14498242 | HCID 14498242 | 88.1% |
Reaction Steps
Into a mixed solvent consisting of 50 ml of acetic acid and 5 ml of water is dissolved 1.4 g of 3-[(2-benzyloxy-3-octadecyloxypropyl)sulfonyl]propyltrimethylammonium mesylate and the solution is shaked in the presence of palladiumcarbon under hydrogen streams. The catalyst is then removed by filtration and the filtrate is concentrated. The resulting residue is treated with acetone to give 1.07 g of the captioned compound as powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04845219 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-fa87d11330624a8fbf433ad2dfabeac3 |
| Source note | uspto-grants-1989_07 |