Trimethylamine → HCID 14498244, compound

Participants

Reaction Steps

Into 6 ml of chloroform are added 1.4 g of 3-[(2-hydroxy-3-octadecyloxypropyl)sulfonyl]propyltrimethylammonium mesylate, 1 ml of methyl isocyanate and 1 ml of trimethylamine and the mixture is shaked overnight at room temperature. The reaction mixture is concentrated under reduced pressure and the residue is purified by silica gel column chromatography to give 0.2 of the captioned

Provenance & Evidence