HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 231263Erstellt: 25. Oktober 2026
Methyl Methanesulfonate → 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium mesylate
https://huagongshe.com/reaction/231263
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | Methyl Methanesulfonate | HCID 4156 | — |
| Edukt | 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine | HCID 14498265 | — |
| Lösungsmittel | Chloroform | HCID 6212 | — |
| Produkt | 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium mesylate | HCID 14498246 | 70,6% |
Reaktionsschritte
In 10 ml of chloroform are dissolved 0.48 g of 2-[(2-methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine and 1 g of methyl methanesulfonate and the solution is stirred at 70° C. for 5 hours. Then the reaction mixture is concentrated under reduced pressure and the residue is crystallized from chloroform and ether to give 417 mg of the captioned compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US04845219 |
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| Quelldatensatz | uspto-grants-1989_07 |
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| ORD ID | ord-1c6f273932834c8c827785532613c3dc |
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| Quellennotiz | uspto-grants-1989_07 |
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