Trimethylamine → HCID 14498262, compound

Participants

Reaction Steps

In 20 ml of toluene containing 4 g of trimethylamine is dissolved 3.1 g of 3-mesyloxypropyl 2-methoxy-3-(3,7,11,15-tetramethylhexadecyloxy)propyl sulfone, and the mixture is stirred at room temperature for 3 days. The reaction mixture is concentrated under reduced pressures to leave a residue which in turn is purified by silica gel column chromatography to yield 2.49 g of the captioned compound.

Provenance & Evidence