Isoprene → HCID 86743224, compound

HRID 231366Notes

Reaction equation

HRID 231366 reaction equation
C1(N)C=CC=CC=1N.[C:9]1([NH2:16])[CH:14]=[CH:13][CH:12]=[C:11]([NH2:15])[CH:10]=1.[CH2:17]=[CH:18][C:19](=[CH2:21])[CH3:20]>CCCCC>[C:9]1([NH2:16])[CH:14]=[CH:13][CH:12]=[C:11]([NH2:15])[CH:10]=1.[CH2:17]=[CH:18][C:19](=[CH2:20])[CH3:21]

Participants

5

Reactant 3

HCID 6557IsopreneHCID 7243O-PhenylenediamineHCID 7935M-Phenylenediamine

Product 1

HCID 86743224HCID 86743224, compound

Reagents, catalysts & solvents 1

HCID 8003PentaneSolvent

Procedure

A 200g (1.85 mol) portion of 1,3-phenylenediamine was alkenylated with 189g (2.77 mol) of isoprene in the same manner as shown in example 10. Product analysis by gas chromatography on isoprene and pentane free sample afforded the following assay.

Sources & evidence

ORD record
ord-d21a3434e0434b2981ada411456b3204
Source dataset
uspto-grants-1989_07
Patent number
US04845291

Reaction notes

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