HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20032349, compound → HCID 20032372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20032349 | HCID 20032349 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 20032372 | HCID 20032372 | 99.3% |
Reaction Steps
N-(2-chloro-4-fluoro-5-nitrobenzyl)-N-methoxyacetamide (1.1 g, 0.0040 mole) was hydrogenated with a small amount (0.1 g) of platinum oxide in 50 ml of acetic acid. The reaction mixture was filtered to leave a solution of 5-[(N-acetyl-N-methoxyamino)methyl]-4-chloro-2-fluoroaniline (0.98 g) dissolved in 50 ml of acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04846882 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-1d96a485caf1452eba510e8197043fd9 |
| Source note | uspto-grants-1989_07 |