Thionyl Chloride → HCID 20032671, compound

Participants

Reaction Steps

20 g of p-(2-methyl-4-n-propylcyclohexyl)-benzoic acid (Examaple 5) is boiled for 1 hour with 24 g of SOCl2, the mixture is evaporated to dryness, the resulting crude acid chloride is dissolved in 150 ml of toluene, to which are added 8 ml of pyridine and 13.2 g of ethylphenol, and the mixture is boiled for 2 hours. Cooling down and customary working up give p-ethylphenyl p-(2-methyl-4-n-propylcyclohexyl)-benzoate.

Provenance & Evidence