HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 20032422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 54547003 | HCID 54547003 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20032422 | HCID 20032422 | — |
Reaction Steps
65 g of POCl3 are added dropwise with stirring at 50° to a solution of 24 g of 2-(p-ethylphenyl)-5-n-propylcyclohexanecarboxamide in 500 ml of DMF. After further stirring for one hour the reaction mixture is poured onto ice and worked up as customary to give 2-(p-ethylphenyl)-5-n-propylcyclohexanecarbonitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04846998 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-24954e7dbbfd46eead6ba1b4c3264c88 |
| Source note | uspto-grants-1989_07 |