HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 231466Generated: October 25, 2026
1,1,3,3-Tetramethyl-disiloxane → 1,3-bis(N-cyclohexyl-3-aminopropyl)-1,1,3,3-tetramethyldisiloxane
https://huagongshe.com/reaction/231466
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,1,3,3-Tetramethyl-disiloxane | HCID 18659 | — |
| Reactant | N-Allylcyclohexylamine | HCID 81115 | — |
| Catalyst | Chloroplatinic acid | HCID 61859 | — |
| Product | 1,3-bis(N-cyclohexyl-3-aminopropyl)-1,1,3,3-tetramethyldisiloxane | HCID 19871404 | — |
Reaction Steps
Following the technique described in Example 1, N-allylcyclohexylamine (0.173 mole), 1,1,3,3-tetramethyldisiloxane (0.0783 mole), and 0.05 g hexachloroplatinic acid are stirred at 70° C. for eight hours at 110° C. under nitrogen. The product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04847154 |
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| Source dataset | uspto-grants-1989_07 |
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| ORD ID | ord-f948b1cae20447918176f84d0a478fbc |
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| Source note | uspto-grants-1989_07 |
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