反应详情

温度

110 °C

Following the technique described in Example 1, N-allylcyclohexylamine (0.173 mole), 1,1,3,3-tetramethyldisiloxane (0.0783 mole), and 0.05 g hexachloroplatinic acid are stirred at 70° C. for eight hours at 110° C. under nitrogen. The product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.

1. distillationThe product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.