HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 73553870, compound → HCID 58051386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 73553870 | HCID 73553870 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58051386 | HCID 58051386 | 83.2% |
Reaction Steps
50 g of 5-methoxy-3-benzofuranacetic acid methylester were dissolved in 200 ml of ethanol, and 18 g of 5% Pd on carbon black (50% water) were added. Hydrogenation was performed at 3 ato. for 4 hours at 65° C. The catalyst was filtered off, and ethanol evaporated yielding 42 g of an oil, which was not further purified before use in the next step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04847254 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-a1916e5f355f43c39f192d5231e4808f |
| Source note | uspto-grants-1989_07 |