Ammonium Hydroxide → HCID 135671361, compound

HRID 231519Notes

Reaction equation

HRID 231519 reaction equation
[CH3:1][C:2]1[C:10]([C:11]#[N:12])=[C:5]2[NH:6][CH2:7][CH2:8][CH2:9][N:4]2[N:3]=1.[OH-:13].[NH4+]>S(=O)(=O)(O)O>[CH3:1][C:2]1[C:10]([C:11]([NH2:12])=[O:13])=[C:5]2[NH:6][CH2:7][CH2:8][CH2:9][N:4]2[N:3]=1

Participants

4

Reactant 2

HCID 14923Ammonium HydroxideHCID 135671370HCID 135671370, compound

Product 1

HCID 135671361HCID 135671361, compound

Reagents, catalysts & solvents 1

HCID 1118Sulfuric AcidSolvent

Procedure

A 1.0 g portion of 4,5,6,7-tetrahydro-2-methylpyrazolo[1,5-a]pyrimidine-3-carbonitrile was dissolved with stirring in 5.0 ml of concentrated sulfuric acid. The mixture was stirred for 6 hours at room temperature then poured onto ice. This mixture was made basic with concentrated ammonium hydroxide and then was filtered to give the product of the example as a colorless solid, mp 234°-236° C.

Workup

  1. additionthen poured onto ice
  2. filtrationwas filtered
  3. customto give the product of the example as a colorless solid, mp 234°-236° C.

Sources & evidence

ORD record
ord-556020a0ce554d488ce70a53369d2bf7
Source dataset
uspto-grants-1989_07
Patent number
US04847256

Reaction notes

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