HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 14297836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 116473-61-1 | HCID 14121778 | — |
| Product | HCID 14297836 | HCID 14297836 | — |
Reaction Steps
In an autoclave, 405 g (2.5 moles) of the 4-(1-methoxy-1-methylethyl)-benzaldehyde obtained according to A, in 200 ml of THF, were flushed several times with nitrogen and hydrogen in the presence of 1 g of ruthenium hydroxide and then hydrogenated at 150° C. and under a hydrogen pressure of 300 bar until the pressure remained constant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04847425 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-3a84274cd7ca4c40a859b34ff1a9f605 |
| Source note | uspto-grants-1989_07 |