HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrazole → HCID 10680030, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrazole | HCID 1048 | — |
| Reactant | 4,6-Dichloropyrimidine | HCID 70943 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10680030 | HCID 10680030 | 84.4% |
Reaction Steps
In anhydrous tetrahydrofuran, 149 mg of 4,6-dichloropyrimidine was substituted with 136 mg of pyrazole. The reaction mixture was treated according to the procedure of Example 1 to yield 179 mg of 2,4-bis(1-pyrazolyl)pyrimidine, recrystallized from n-hexane, the compound had a melting point of 152°-153° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04849424 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-fc07d3ffe552458fae90f246f23e6390 |
| Source note | uspto-grants-1989_07 |