HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 10725947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 4-chloro-2-(1H-imidazol-1-yl)pyrimidine | HCID 10607483 | — |
| Product | HCID 10725947 | HCID 10725947 | — |
Reaction Steps
Following the procedure of Example 15, 180 mg of 4-chloro-2-(1-imidazolyl)pyrimidine were reacted with 23 mg of sodium metal and 2 ml of anhydrous methanol was carried out to yield 134 mg of 2-(1-imidazolyl)-4-methoxypyrimidine, having a melting point of 78°-79° C., recrystallized from a mixture of n-hexane and ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04849424 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-eb5c83754db84ac184d5b230752f497a |
| Source note | uspto-grants-1989_07 |