Dichloromethane → 3-Iodo-8-nitro-1,3,4,5-tetrahydro-benzo[b]azepin-2-one

HRID 2319731Notes

Reaction equation

HRID 2319731 reaction equation
[CH2:30]([Cl:31])[Cl:32].[CH3:16][N:17]([CH3:18])[CH2:19][CH2:20][N:21]([CH3:22])[CH3:23].[I:24][Si:25]([CH3:26])([CH3:27])[CH3:28].[I:29].[N+:1](=[O:2])([O-:3])[c:4]1[cH:5][c:6]2[c:7]([cH:14][cH:15]1)[CH2:8][CH2:9][CH2:10][C:11](=[O:13])[NH:12]2>>[N+:1](=[O:2])([O-:3])[c:4]1[cH:5][c:6]2[c:7]([cH:14][cH:15]1)[CH2:8][CH2:9][CH:10]([I:24])[C:11](=[O:13])[NH:12]2

Participants

6

Reactant 5

HCID 6344DichloromethaneHCID 8037N,N,N',N'-TetramethylethylenediamineHCID 24841Hydrogen iodideHCID 85247Trimethylsilyl iodideHCID 40932148-Nitro-1,3,4,5-tetrahydro-2H-1-benzazepin-2-one

Product 1

HCID 672634303-Iodo-8-nitro-1,3,4,5-tetrahydro-benzo[b]azepin-2-one

Sources & evidence

ORD record
ord-a807fd6203ec4a6dbd1c41e402f354ee
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (10/10)

Reaction notes

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