HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylamine → HCID 20030583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylamine | HCID 7912 | — |
| Reactant | 2-Cyanopyridine-3-carboxylic acid | HCID 12535315 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20030583 | HCID 20030583 | 99.5% |
Reaction Steps
2-Cyanonicotinic acid (0.74 g; 0.005 mol) suspended in acetone (40 cc) is treated with diisopropylamine (0.56 g; 0.0056 mol). The solvent is then evaporated off and the residue is crystallized in hexane: diisopropylammonium 2-cyanonicotinate (1.24 g; m.p. 156.7° C.) is obtained (yield=99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851396 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-aa3f32fd1b9d454e8391ba49a20f808d |
| Source note | uspto-grants-1989_07 |