Dichloromethane → 1,9-Dichloro-3-methyl-7-phenyl-5H-pyrimido[4,5-d][2]benzazepine

HRID 2320286Notes

Reaction equation

HRID 2320286 reaction equation
[CH2:30]([Cl:31])[Cl:32].[Cl:1][c:2]1[cH:3][c:4]2[c:5]([cH:23][cH:24]1)-[c:6]1[c:7]([n:17][c:18]([CH3:22])[nH:19][c:20]1=[O:21])[CH2:8][N:9]=[C:10]2[c:11]1[cH:12][cH:13][cH:14][cH:15][cH:16]1.[P:25]([Cl:26])([Cl:27])([Cl:28])=[O:29]>>[Cl:1][c:2]1[cH:3][c:4]2[c:5]([cH:23][cH:24]1)-[c:6]1[c:7]([n:17][c:18]([CH3:22])[n:19][c:20]1[Cl:27])[CH2:8][N:9]=[C:10]2[c:11]1[cH:12][cH:13][cH:14][cH:15][cH:16]1

Participants

4

Reactant 3

HCID 6344DichloromethaneHCID 24813Phosphorus oxychlorideHCID 135759068HCID 135759068, compound

Product 1

HCID 132717911,9-Dichloro-3-methyl-7-phenyl-5H-pyrimido[4,5-d][2]benzazepine

Sources & evidence

ORD record
ord-46b6b280195b42e9be7bf3ae6444e4f9
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (10/10)

Reaction notes

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