HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20030629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phenylacetone | HCID 7678 | — |
| Reactant | HCID 19780113 | HCID 19780113 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20030629 | HCID 20030629 | — |
Reaction Steps
4.8 g. (20 mmole) 6-(4-hydrazinophenyl)-2,3,4,5-tetrahydropyridazin-3-one hydrochloride (according to Example 2 (a)) are suspended in 75 ml. 2N hydrochloric acid and 75 ml. ethanol, mixed with 2.8 g. (21 mmole) phenylacetone, stirred for 3 hours at 25° C., filtered off with the suction and the title compound obtained is recrystallised from methanol. Yield 4.85 g. (80% of theory); m.p. 297°-299° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04851406 |
| Source dataset | uspto-grants-1989_07 |
| ORD ID | ord-7d317507304d4c5fb086e4ced882c8c8 |
| Source note | uspto-grants-1989_07 |